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Comparing Thermal Conductivity Methods

 

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Steady-State Methods for Measuring Thermal Conductivity

 

Steady-state methods apply a heat source continuously to a sample. They are considered the traditional standard in some applications, such as the Guarded Hot Plate method for building materials. While these methods can be highly accurate, they often often requires large samples, exacting preparation to conform to ISO standards, and long test times. These constraints make steady-state methods challenging to apply against liquids, high-thermal conductivity materials, or smaller samples, such as films or slab-like materials.

Common steady-state methods include:

  • Guarded Hot Plate (ASTM C177)
  • Heat Flow Meter (ASTM C518)
  • Guarded-Comparative–Longitudinal Heat Flow Meter (ASTM E1225)
  • Comparative-Axial-Heat-Flow (Cut-Bar) Method

Transient Methods for Measuring Thermal Conductivity

Transient methods apply the heat source momentarily  and monitors the temperature progression through time, which dramatically reduces test cycle times (minutes versus hours). Over the past three decades, transient methods have been the preferred approach versus steady-state for many researchers due to their speed, flexibility, and smaller sample requirements.

The 2nd Edition highlights the following core transient methods:

  • Modified Transient Plane Source (MTPS): (ASTM D7984)
  • Transient Plane Source (TPS): (ISO 22007-2 and GB/T 32064)
  • Transient Line Source (TLS): (ASTM D5334 and D5930)
  • Transient Hot Wire (THW): (ISO 22007-4)

Additional Methods Covered in the 2nd Edition (Educational Overview)

To provide a complete picture of the thermal conductivity testing landscape, the guide also includes educational overviews of other methods not part of Trident, such as:

  • Single-Sided TPS
  • Laser Flash Diffusivity (LFA): (ASTM E1461)
  • Frequency-Domain Thermoreflectance / Time-Domain Thermoreflectane (FDTR/TDTR)
  • 3-omega

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Comparing Thermal Conductivity Methods

Compare Method

Modified Transient Plane Source

Transient Line Source

Transient Plane Source

Guarded Hot Plate / Heat Flow Meter

Laser Flash Diffusivity

SPEED & FLEXIBILITY

Sample Preparation None Required None Required Some Extensive Extensive
Testing Time Seconds Minutes Minutes Hours Hours
Training Time Minimal Minimal Significant Moderate Moderate
Non-Destructive Yes Yes No No No
Method Development
ASTM/ISO Standards ASTM D7984, WK50791, WK43689 ASTM D5334, D5930, IEEE442 ISO-22007-2,

GB/T 32064

ASTM C518, C177 ASTM E1461, E2585

RANGE

k-Range (W/mK) 0 – 500 0.1 – 6 0.005 – 2000 (requires Cρ) 0 – 2 0 – 500 (requires density & Cρ)

SAMPLE CONFIGURATION

Minimum 0 – 500 80 ml Two Identical Samples 6” x 6” (150 x 150mm) 0.5” diameter (12.4mm) 0.004” thick (1mm)
Maximum Unlimited (17mm) Unlimited Two Identical Samples Unlimited 24” x 24” (600 x 600mm) 0.5” diameter (12.4mm) 0.004” thick (1mm)
Material Testing Capability Solids, Liquids, Powders, Pastes Granular Materials, Powders, Slurries, Gels, and Pastes Solids Solids Solids
Isotropic & Anisotropic Materials Yes No Yes (Requires Cρ and Density) No Yes
Heterogeneous Materials Yes No Yes No No
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